Monday, February 17, 2014

Stability Studies May Lead to Instability - Food Scientist Life



This is a series of posts in which I share snippets of what it's like to be a food scientist. As a product developer for dry powder shakes, there are some lessons I never learned in school and some challenges I never saw coming.


Green-Eyed Insight on Stability Studies
Have you ever looked at an expiration date and wondered, "How do they know?" Determining or confirming the shelf-life of a product is important for several reasons, but the process itself can be a bit mind-numbing. Here's what I didn't learn in school.


Why It's Important
Expiration dates are based on the answers to several different questions. When does the product become unpalatable? When do the vitamins and minerals degrade below the amounts on the label? When does the product become unsafe to eat? To sell a product that meets consumer sensory expectations, label claims and food safety requirements, you have to know the answers to all three questions. 


Side-note: Why It's Confusing
This would be a great time to note that expiration dates can be perplexing. An expiration date is not quite the same as the "sell by", "use by" or "best by" date. For example, "use by" is meant to help consumers know when a product is no longer good to eat whereas "best by" and "sell by" are meant to help those selling the product manage their stock (think of those racks of discounted "Manager's Special" items in back of the grocery store). Misinterpretation of these dates leads to as much as $165 billion in food waste PER YEAR according to a report by the Harvard Food Law and Policy Clinic and the National Resources Defense Council [1, 2].

Why It's Complicated

As a product developer, I work on a dry powder shake that's supposed to last one year. Our products don't use the "best by" or "use by" terms; our packages say "EXP MM/DD/YYYY". Up until that date, our product is expected to taste as delicious as the day it was made, and must provide all the vitamins/mineral and nutrient contents on the label. This is harder than it seems because flavors, proteins, vitamins/minerals and oxidation-prone (air-sensitive) ingredients like fish oil, chia and flax all have different rates of degradation. In some cases, products start out with vitamin/mineral overages so there's enough left at the end of shelf-life to meet the label claims. Instead of using overages, you might shorten the shelf-life or slow the degradation of certain nutrients with encapsulation [3].

How We Do It Here
In order to continuously improve the food safety and quality of our finished product, my team and I are always looking at alternate ingredients. For example, say blueberry powder A is great, but blueberry powder B is cheaper and has lower heavy metal contents. We can't just switch from one to another; what if blueberry powder B makes the product taste funny after 6 months? Our product is supposed to be delicious and nutritious for a whole year. We've got to test this. 

Food science stability studies
500 servings x 35g each x 4 variants
Step One: Make your blends. 
For your control and all your variants you need to make a big enough batch to put a few servings into the freezer ("time zero"), a few servings into room temperature storage, and a few servings into accelerated storage (where 1 week at 40* Celsius is equivalent to 2 months at room temp). Accelerated storage is a marvelous tool because it only takes six weeks to determine how the product will taste after one year in real time. Plus, since my office is always freezing cold, I rather enjoy fetching samples from accelerated storage and feeling the hot air hit my face.
 
break big tasks into small steps



Step Two: Divvy your blends up into single pouches. 
Warning – this may take a while, depending on the size of your batches and number of variants. Unless you have Audible or music or some metaphysical question to ponder you may feel your mind slipping a little. Fight the urge to listen to podcasts because you need to pay attention to what you're doing. I swore off listening to Baseball Tonight and "Wait Wait …Don't Tell Me" because once I lost track of what sample I was working on and had to start over. Rookie mistake.

Step Three: Seal your pouches. 
Make darn sure they're sealed. There's nothing worse than putting all the time and energy into preparing samples then seeing random powder piles on the shelves inside the stability chamber.

Plastic bags and small boxes come in handy!
Step Four: Set calendar reminders.
Include specifics on what samples to pull, from what location (freezer, room temp, accelerated) on which days. Even though you've put all this work into setting up the stability study, it's not uncommon to set it and forget it. Putting the samples in the Hot Box mentally feels like the job is done – no more Open Loops. Since one week in the 40*C chamber is the equivalent of two months, it's important not to miss the days you're supposed to pull a sample.

Step Five: Taste. 
This might be a mentally exhausting exercise based on the number of samples you have to pull. Unlike Pavlov's dogs you might grow to dread the sound of the calendar reminder, especially if there's a lot of samples or if they're not aging well. This is where oyster crackers and carbonated water come in handy – see previous post.

Bottom Line

Shelf-life and stability studies can be mind-numbing, tedious, time-consuming experiments, but you'll learn more about your ingredients and your product than you could possibly anticipate. It's kind of exciting to have that knowledge that others aren't privy to, and that knowledge improves your product and your skill set as a product developer. That is the silver lining.


Resources:
[2] NRDC: "The Dating Game: How Confusing Food Date Labels Lead to Food Waste in America" http://www.nrdc.org/food/expiration-dates.asp
[3] Maxx Performance Newsletter – Winter 2014 http://email.maxxperform.com/t/ViewEmail/y/B1F4EE53EC2CEA20

Related Posts:

 

Next Lesson - "The Linger": A Food Science Horror Story
___________________________________________________

Stay tuned for more lessons from the lab. 
Follow GreenEyedGuide on Twitter

1 comment:

  1. Here's another great article on food waste: http://feedstuffsfoodlink.com/story-food-waste-has-750b-impact-71-102409

    ReplyDelete